Research Title |
Preparation and characterization of CaCu3Ti4O12 materials by
sol-gel process |
Date of Distribution |
1 May 2016 |
Conference |
Title of the Conference |
The Pure and Applied Chemistry International Conference 2016 (PACCON2016) |
Organiser |
The Chemical Society of Thailand under the Patronage of Professor Dr. HRH Princess Chulabhorn |
Conference Place |
Bangkok International Trade and Exhibition Centre (BITEC) |
Province/State |
Bangkok, Thailand |
Conference Date |
9 February 2016 |
To |
11 February 2016 |
Proceeding Paper |
Volume |
2016 |
Issue |
1 |
Page |
783-786 |
Editors/edition/publisher |
Tirayut Vilaivan |
Abstract |
CaCu3Ti4O12 (CCTO) powders were prepared by sol-gel process using acetic acid as a solvent and also as cross-linking agent by varying the mole ratio of metal and acetic acid
(1:40, 1:50 and 1:60) and calcining temperature (600–900 ºC) for 3 h. The dried gels were
characterized by TG-DTA and FT-IR techniques. The sintered samples were characterized by
FT-IR, XRD, SEM techniques and impedance analyzer for dielectric properties measurement.
All samples showed CCTO perovskite structure with small amounts of TiO2 and CuO phases.
From optimizing conditions for the preparation process, acetic acid with the mole ratio of
1:40 was preferably used as a solvent and a cross-linking agent for preparing CCTO. For the
sintered pellet samples calcined at different temperatures, all samples showed the high
dielectric constant (εr) ∼103 – 104 and very low loss tangent (tanδ) ∼0.03–0.05 at 1 kHz. The lowest tanδ (0.03) was found in the CCTO calcined at 800 ºC and its εr at 1 kHz was 8.24×103
.
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Author |
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Peer Review Status |
มีผู้ประเมินอิสระ |
Level of Conference |
นานาชาติ |
Type of Proceeding |
Full paper |
Type of Presentation |
Poster |
Part of thesis |
true |
Presentation awarding |
false |
Attach file |
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Citation |
0
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