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             Publication
Journal Publication
Research Title Preparation and characterization of CaCu3Ti4O12 materials by sol-gel process  
Date of Distribution 1 May 2016 
Conference
     Title of the Conference The Pure and Applied Chemistry International Conference 2016 (PACCON2016) 
     Organiser The Chemical Society of Thailand under the Patronage of Professor Dr. HRH Princess Chulabhorn 
     Conference Place Bangkok International Trade and Exhibition Centre (BITEC) 
     Province/State Bangkok, Thailand 
     Conference Date 9 February 2016 
     To 11 February 2016 
Proceeding Paper
     Volume 2016 
     Issue
     Page 783-786 
     Editors/edition/publisher Tirayut Vilaivan  
     Abstract CaCu3Ti4O12 (CCTO) powders were prepared by sol-gel process using acetic acid as a solvent and also as cross-linking agent by varying the mole ratio of metal and acetic acid (1:40, 1:50 and 1:60) and calcining temperature (600–900 ºC) for 3 h. The dried gels were characterized by TG-DTA and FT-IR techniques. The sintered samples were characterized by FT-IR, XRD, SEM techniques and impedance analyzer for dielectric properties measurement. All samples showed CCTO perovskite structure with small amounts of TiO2 and CuO phases. From optimizing conditions for the preparation process, acetic acid with the mole ratio of 1:40 was preferably used as a solvent and a cross-linking agent for preparing CCTO. For the sintered pellet samples calcined at different temperatures, all samples showed the high dielectric constant (εr) ∼103 – 104 and very low loss tangent (tanδ) ∼0.03–0.05 at 1 kHz. The lowest tanδ (0.03) was found in the CCTO calcined at 800 ºC and its εr at 1 kHz was 8.24×103 .  
Author
567020051-1 Miss WIRINRATCH SUE-AOK [Main Author]
Science Doctoral Degree

Peer Review Status มีผู้ประเมินอิสระ 
Level of Conference นานาชาติ 
Type of Proceeding Full paper 
Type of Presentation Poster 
Part of thesis true 
Presentation awarding false 
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